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CLEANING.TXT
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1994-11-01
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The final operation after fabrication or heat treatment is cleaning to
remove surface contamination and restore corrosion resistance of the
exposed surfaces. Degreasing to remove cutting oils, grease, crayon
markings, fingerprints, dirt, grime and other organic residues is the
first step.
Degreasing: Non-chlorinated solvents should be used in order to avoid
leaving residues of chloride ions in crevices and other locations where
they can initiate crevice attack, pitting, and/or stress corrosion
later on when the equipment is placed in service.
Machined components: After degreasing, machined components are
sometimes "passivated" in 10% nitric acid. Nitric acid enhances the
natural oxide surface film.
Fabrications: After degreasing, metallic surface contaminants such as
iron embedded in fabrication shop forming and handling, weld splatter,
heat tint, inclusions and other metallic particles must be removed in
order to restore the inherent corrosion resistance of the stainless
steel surface.
Nitric-HF pickling, (10% HNO3, 2% HF at 49C to 60C (120 to 140F), is
the most widely used and effective method removing metallic surface
contamination. Pickling may be done by immersion or locally using a
pickling paste.
Electropolishing, using oxalic or phosphoric acid for the electrolyte
and a copper bar or plate for the cathode can be equally effective.
Electro-polishing may be done locally to remove heat tint alongside
of welds or over the whole surface.
Both pickling and electropolishing remove a layer several atoms deep
from the surface. Removal of the surface layer has the further benefit
of removing surface layers that may have become somewhat impoverished
in chromium during the final heat treatment operation.
Glass bead or walnut shell blasting are very effective in removing
metallic surface contamination without damaging the surface. It is
sometimes necessary to resort to blasting with clean sand to restore
heavily contaminated surfaces such as tank bottoms, but care must be
taken to be certain the sand is truly clean, is not recycled and does
not roughen the surface. Steel shot blasting should not be used as it
will contaminate the stainless steel with an iron deposit.
Stainless steel wire brushing or light grinding with clean aluminum
oxide abrasive discs or flapper wheels are helpful. Grinding or
polishing with grinding wheels or continuous belt sanders tend to
overheat the surface layers to the point where resistance cannot be
fully restored even with subsequent pickling.
More information on cleaning and finishing may be found in:
"Heat Treating, Cleaning and Finishing", Metals Handbook,
10th Edition.
ASTM A 380, "Recommended Practice for Cleaning and Descaling
Stainless Steel Parts, Equipment and Systems", ASTM,
1916 Race Street, Philadelphia, PA 19103.
Tuthill, A. H., "Fabrication and Post Fabrication Cleanup of
Stainless Steel", NiDI literature, Item 10 004.
Pettibone, J. S., "Burgers, Fries, Coke, and Stainless Steel"
NiDI literature, Item 10 009.
AISI, "Cleaning and Descaling Stainless Steel", NiDI literature,
Item 9 001.