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- +------------------------------------+
- ! KING ARTHUR'S DEMOLITION ARTICLE #1!
- +------------------------------------+
-
-
- LIKE ALL CHEMISTS I MUST ADVISE
- YOU ALL TO TAKE THE GREATEST CARE AND
- CAUTION WHEN YOU ARE DOING THIS. EVEN
- IF YOU HAVE MADE THIS STUFF BEFORE.
-
- THIS FIRST ARTICLE WILL GIVE YOU
- INFORMATION ON MAKING NITROGLYERIN, THE
- BASIC INGREDIENT IN A LOT OF EXPLOSIVES
- SUCH AS STRAIGHT DYNAMITES, AND GELETIN
- DYNAMITES.
-
- --------------------------------------
-
- MAKING NITROGLYCERIN
-
- --------------------------------------
-
-
- 1. FILL A 75-MILLILITER BEAKER TO
- THE 13 ML. LEVEL WITH FUMING RED NITRIC
- ACID, OF 98% PURE CONCENTRATION.
-
- 2. PLACE THE BEAKER IN AN ICE BATH
- AND ALLOW TO COOL BELOW ROOM TEMP.
-
- 3. AFTER IT HAS COOLED, ADD TO IT
- THREE TIMES THE AMOUNT OF FUMING
- SULFERIC ACID (99% H2SO4). IN OTHER
- WORDS, ADD TO THE NOW-COOL FUMING
- NITRIC ACID 39 ML. OF FUMING SULFERIC
- ACID. WHEN MIXING ANY ACIDS, ALWAYS DO
- IT SLOWLY AND CAREFULLY TO AVOID
- SPLATTERING.
-
- 4. WHEN THE TWO ARE MIXED, LOWER
- THIER TEMP. BY ADDING MORE ICE TO THE
- BATH, ABOUT 10-15 DEGREES CENTIGRADE.
- (USE A MERCURY-OPERATED THERMOMETER)
-
- 5. WHEN THE ACID SOLUTION HAS
- COOLED TO THE DESIRED TEMPERATURE, IT
- IS READY FOR THE GLYCERIN. THE GLYCERIN
- MUST BE ADDED IN SMALL AMOUNTS USING A
- MEDICINE DROPPER. (READ THIS STEP
- ABOUT 10 TIMES!) GLYCERIN IS ADDED
- SLOWLY AND CAREFULLY (I MEAN CAREFUL!)
- UNTIL THE ENTIRE SURFACE OF THE ACID IT
- COVERED WITH IT.
-
- 6. THIS IS A DANGEROUS POINT SINCE
- THE NITRATION WILL TAKE PLACE AS SOON
- AS THE GLYCERIN IS ADDED. THE NITRATION
- WILL PRODUCE HEAT, SO THE SOLUTION MUST
- BE KEPT BELOW 30 DEGREES CENTIGRADE! IF
- THE SOLUTION SHOULD GO ABOVE 30
- DEGREES, IMMEDIATELY DUMP THE SOLUTION
- INTO THE ICE BATH! THIS WILL INSURE
- THAT IT DOES NOT GO OFF IN YOUR FACE!
-
- 7. FOR HTE FIRST TEN MINUTES OF
- NITRATION, THE MIXTURE SHOULD BE GENTLY
- STIRRED. IN A NORMAL REACTION THE
- NITROGLYCERIN WILL FORMAS A LAYER ON
- TOP OF THE ACID SOLUTION, WHILE THE
- SULFERIC ACID WILL ABSORB THE EXCESS
- WATER.
-
- 8. AFTER THE NITRATION HAS TAKEN
- PLACE, AND THE NITROGLYCERIN HAS FORMED
- ON THE TOP OF THE SOLUTION, THE ENTIRE
- BEAKER SHOULD BE TRANSFERRED SLOWLY AND
- CAREFULLY TO ANOTHER BEAKER OF WATER.
- WHEN THIS IS DONE THE NITROGLYCERIN
- WILL SETTLE AT THE BOTTEM SO THE OTHER
- ACIDS CAN BE DRAINED AWAY.
-
- 9. AFTER REMOVING AS MUCH ACID AS
- POSIBLE WITHOUT DISTURBING THE
- NITROGLYCERIN, REMOVE THE NITROGLYCERIN
- WITH AN EYEDROPPER AND PLACE IT IN A
- BICARBONATE OF SODA (SODIUM BICARBONATE
- IN CASE YOU DIDN'T KNOW) SOLUTION. THE
- SODIUM IS AN ALKALAI AND WILL
- NUETRALIZE MUCH OF THE ACID REMAINING.
- THIS PROCESS SHOULD BE REPEATED AS MUCH
- AS NECESARRY USING BLUE LITMUS PAPER TO
- CHECK FOR THE PRESENCE OF ACID. THE
- REMAINING ACID ONLY MAKES THE NITROGLY-
- CERIN MORE UNSTABLE THAN IT ALREADY
- IS.
-
- 10. FINALLY! THE FINAL STEP IS TO
- REMOVE THE NITROGLYCERIN FROM THE BI-
- CARBONATE. HIS IS DONE WITH AND EYE-
- DROPPER, SLOWLY AND CAREFULLY. THE
- USUAL TEST TO SEE IF NITRATION HAS BEEN
- SUCCESSFUL IS TO PLACE ONE DROP OF THE
- NITROGLYCERIN ON METAL AND IGNITE IT.
- IF IT IS TRUE NITROGLYCERIN IT WILL
- BURN WITH A CLEAR BLUE FLAME.
-
- ** CAUTION **
- NITRO IS VERY SENSATIVE TO DECOMPOSI-
- TION, HEATING DROPPING, OR JARRING, AND
- MAY EXPLODE IF LEFT UNDISTURBED AND
- COOL.
-
- --------------------------------------
-
- NEXT ARTICLES: #2 MERCURY FULMINATE
- #3 DYNAMITES
- #4 CHLORIDE OF AZODE
-
- --------------------------------------
- SPECIAL THANKS TO THE ICEBERG <=-:+**#
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